{"id":33817,"date":"2025-06-17T08:44:29","date_gmt":"2025-06-17T06:44:29","guid":{"rendered":"https:\/\/georganics.sk\/research\/continuous-preparation-of-arylmagnesium-reagents-in-flow-with-inline-ir-monitoring\/"},"modified":"2025-06-30T13:49:40","modified_gmt":"2025-06-30T11:49:40","slug":"continuous-preparation-of-arylmagnesium-reagents-in-flow-with-inline-ir-monitoring","status":"publish","type":"page","link":"https:\/\/georganics.sk\/de\/research\/continuous-preparation-of-arylmagnesium-reagents-in-flow-with-inline-ir-monitoring\/","title":{"rendered":"Continuous Preparation of Arylmagnesium Reagents in Flow with Inline IR Monitoring"},"content":{"rendered":"

Eine neu entwickelte mikroskalige ReactIR-Durchflusszelle wurde als praktisches und vielseitiges Inline-Analysetool f\u00fcr die Grignard-Bildung in kontinuierlichen chemischen Prozessen eingesetzt. Die LiCl-vermittelte Halogen-\/Mg-Austauschreaktion wurde zur Herstellung funktionalisierter Arylmagnesiumverbindungen aus Aryliodiden oder -bromiden genutzt. Dar\u00fcber hinaus wurde die Inline-IR-\u00dcberwachung zur Analyse der Umwandlung und m\u00f6glicher Nebenproduktbildung sowie als potenzielles Instrument zur Aufkl\u00e4rung mechanistischer Details eingesetzt. Die hier beschriebenen Ergebnisse zeigen, dass die kontinuierlichen Durchflusssysteme<\/a> aufgrund der schnellen Durchmischung und effizienten W\u00e4rme\u00fcbertragung f\u00fcr stark exotherme Reaktionen wie die Grignard-Austauschreaktion geeignet sind.<\/p>\n","protected":false},"excerpt":{"rendered":"

Eine neu entwickelte mikroskalige ReactIR-Durchflusszelle wurde als praktisches und vielseitiges Inline-Analysetool f\u00fcr die Grignard-Bildung in kontinuierlichen chemischen Prozessen eingesetzt. Die LiCl-vermittelte Halogen-\/Mg-Austauschreaktion wurde zur Herstellung funktionalisierter Arylmagnesiumverbindungen aus Aryliodiden oder -bromiden genutzt. Dar\u00fcber hinaus wurde die Inline-IR-\u00dcberwachung zur Analyse der Umwandlung und m\u00f6glicher Nebenproduktbildung sowie als potenzielles Instrument zur Aufkl\u00e4rung mechanistischer Details eingesetzt. Die hier […]<\/p>\n","protected":false},"author":6,"featured_media":0,"parent":18990,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"template-randpost.php","meta":{"_acf_changed":false,"footnotes":""},"folder":[],"class_list":["post-33817","page","type-page","status-publish","hentry"],"acf":[],"yoast_head":"\nContinuous Preparation of Arylmagnesium Reagents in Flow with Inline IR Monitoring - Georganics<\/title>\n<meta name=\"description\" content=\"Kontinuierliche Durchflusssysteme sind f\u00fcr stark exotherme Reaktionen wie die Grignard-Austauschreaktion effektiv.\" \/>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/georganics.sk\/de\/research\/continuous-preparation-of-arylmagnesium-reagents-in-flow-with-inline-ir-monitoring\/\" \/>\n<meta property=\"og:locale\" content=\"de_DE\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Continuous Preparation of Arylmagnesium Reagents in Flow with Inline IR Monitoring\" \/>\n<meta property=\"og:description\" content=\"Kontinuierliche Durchflusssysteme sind f\u00fcr stark exotherme Reaktionen wie die Grignard-Austauschreaktion effektiv.\" \/>\n<meta property=\"og:url\" content=\"https:\/\/georganics.sk\/de\/research\/continuous-preparation-of-arylmagnesium-reagents-in-flow-with-inline-ir-monitoring\/\" \/>\n<meta property=\"og:site_name\" content=\"Georganics\" \/>\n<meta property=\"article:modified_time\" content=\"2025-06-30T11:49:40+00:00\" \/>\n<meta name=\"twitter:card\" content=\"summary_large_image\" \/>\n<meta name=\"twitter:label1\" content=\"Gesch\u00e4tzte Lesezeit\" \/>\n\t<meta name=\"twitter:data1\" content=\"1\u00a0Minute\" \/>\n<script type=\"application\/ld+json\" class=\"yoast-schema-graph\">{\"@context\":\"https:\\\/\\\/schema.org\",\"@graph\":[{\"@type\":\"WebPage\",\"@id\":\"https:\\\/\\\/georganics.sk\\\/de\\\/research\\\/continuous-preparation-of-arylmagnesium-reagents-in-flow-with-inline-ir-monitoring\\\/\",\"url\":\"https:\\\/\\\/georganics.sk\\\/de\\\/research\\\/continuous-preparation-of-arylmagnesium-reagents-in-flow-with-inline-ir-monitoring\\\/\",\"name\":\"Continuous Preparation of Arylmagnesium Reagents in Flow with Inline IR Monitoring - 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